原理:試樣用乙睛提取，提取液經(jīng)固相萃取成分散固相萃取凈化，植物油試樣經(jīng)凝膠滲透色譜凈化,氣相色譜-質(zhì)譜聯(lián)用儀檢測(cè),內(nèi)標(biāo)法或外標(biāo)法定量.（點(diǎn)擊圖片查看標(biāo)準(zhǔn)詳情）
原理:試樣用乙睛提取，提取液經(jīng)固相萃取成分散固相萃取凈化，植物油試樣經(jīng)凝膠滲透色譜凈化,氣相色譜-質(zhì)譜聯(lián)用儀檢測(cè),內(nèi)標(biāo)法或外標(biāo)法定量.
| 水 |
| 一級(jí)水 |
| 乙腈 |
| CH3CN,75-05-8,分析純 |
| 乙酸乙酯 |
| CH3COOCH2CH3,141-78-6,色譜純 |
| 甲苯 |
| C7H8,108-88-3,色譜純 |
| 環(huán)己烷 |
| C6H12,110-82-7 ,色譜純 |
| 氯化鈉 |
| NaCl,7647-14-5 ,分析純 |
| 乙酸鈉 |
| 醋酸鈉,CH3COONa,127-09-3,分析純 |
| 乙酸 |
| 醋酸,CH3COOH, 64-19-7,分析純 |
| 硫酸鎂 |
| MgSO4,7487-88-9 ,分析純 |
| 檸檬酸鈉 |
| Na3C6H5O7,68-04-2,分析純 |
| 檸檬酸氫二鈉 |
| 6H6NA2O7,18996-35-5 ,6132-05-4,分析純 |
| 冰箱 |
| -18℃ |
| 冰箱 |
| 0℃-4℃ |
| 容量瓶 |
| 250 mL |
| 容量瓶 |
| 10mL |
| 樣品篩 |
| 425μm的標(biāo)準(zhǔn)網(wǎng)篩 |
| 聚乙烯瓶 |
| 或袋 |
| 環(huán)氧七氯B |
| 內(nèi)標(biāo),Heptachlor epoxide (Isomer B),1024-57-3,純度≥95% |
| 固相萃取柱 |
| 石墨化炭黑-氨基復(fù)合柱,500mg/500mg,容積6mL |
| 乙二胺-N-丙基硅烷化硅膠 |
| PSA,40μm~60μm |
| 十八烷基硅烷鍵合硅膠 |
| C18,40μm~60μm |
| 石墨化碳黑 |
| GCB,40μm~120μm |
| 均質(zhì)子 |
| 陶瓷,2cm(長)×1cm(外徑) |
| 濾膜 |
| 微孔濾膜（有機(jī)相）,13mm×0.22μm |
| 氣相色譜串聯(lián)質(zhì)譜儀 |
| 氣相色譜三重四極桿質(zhì)譜聯(lián)用儀，配有電子轟擊源(EI) |
| 凝膠滲透色譜儀 |
| 配有25mm(內(nèi)徑)X500mm,內(nèi)裝Bio- Beads SX-3填料或相當(dāng)?shù)膬艋?/td> |
| 天平 |
| 分析天平,感量0.1mg和0.01g |
| 勻漿機(jī) |
| 高速，轉(zhuǎn)速不低于15000r/min |
| 離心機(jī) |
| 轉(zhuǎn)速不低于4200r/min |
| 搗碎機(jī) |
| 組織搗碎機(jī) |
| 旋轉(zhuǎn)蒸發(fā)儀 |
| – |
| 氮吹儀 |
| 可控溫,40℃ |
| 振蕩器 |
| 渦旋振蕩器 |
| 離心管 |
| 15mL塑科 |
| 雞心瓶 |
| 150mL |
| 離心管 |
| 100ml塑料 |
| 離心管 |
| 塑料,50ml |
| 試管 |
| 10ml |
| 雞心瓶 |
| 100ml茄形瓶 |
| 樣品瓶 |
| 10mL |
| 離心管 |
| 10mL玻璃離心管 |
| 貯液器 |
| 50ml儲(chǔ)液器 |
| 氮?dú)?/td> |
| – |
| 氣相色譜柱 |
| 14%腈丙基苯基-86%二甲基聚硅氧烷,30m×0.25mm×0.25μm,或相當(dāng)者 |
| 氦氣 |
| 載氣,純度≧99.999% |
附 錄 A (資料性附錄) 208種農(nóng)藥及其代謝物中英文名稱和定量限
| 乙酰甲胺磷 |
| acephate,30560-19-1,純度≥95% |
| 乙草胺 |
| Acetochlor,34256-82-1,純度≥95% |
| 苯草醚 |
| aclonifen,74070-46-5,純度≥95% |
| 甲草胺 |
| alachlor,15972-60-8,純度≥95% |
| 烯丙菊酯 |
| Allethrin,584-79-2,純度≥95% |
| α-六六六 |
| α-BHC,319-84-6,純度≥95% |
| α-硫丹 |
| Endosulfan (a-isomer),959-98-8,純度≥95% |
| 莎稗磷 |
| Anilofos,64249-01-0,純度≥95% |
| 脫乙基阿特拉津 |
| atrazine-desethyl,6190-65-4,純度≥95%,脫乙基莠去津 |
| β-硫丹 |
| Endosulfan (β-isomer),33213-65-9,純度≥95% |
| 聯(lián)苯菊酯 |
| Bifenthrin,82657-04-3,純度≥95% |
| 啶酰菌胺 |
| boscalid,188425-85-6,純度≥95% |
| 除草定 |
| Bromacil,314-40-9,純度≥95% |
| 溴苯烯磷 |
| Bromfenvinfos,33399-00-7,純度≥95% |
| 溴硫磷 |
| Bromofos,2104-96-3,純度≥95% |
| 溴螨酯 |
| bromopropylate,18181-80-1,純度≥95% |
| 乙嘧酚磺酸酯 |
| bupirimate,41483-43-6,純度≥95% |
| 三硫磷 |
| Carbofenothion,786-19-6,純度≥95% |
| 蟲螨磷 |
| chlorthiophos,純度≥95% |
| 環(huán)草敵 |
| cycloate,1134-23-2,純度≥95% |
| 環(huán)氟菌胺 |
| Cyflufenamid,180409-60-3,純度≥95% |
| 氯氰菊酯 |
| cypermethrin,52315-07-8，純度≥95% |
| 脫葉磷 |
| DEF,78-48-8,純度≥95% |
| 溴氰菊酯 |
| deltamethrin,52918-63-5,純度≥95% |
| 除線磷 |
| dichlofenthion,97-17-6,純度≥95% |
| 敵草腈 |
| Dichlobenil,1194-65-6,純度≥95% |
| 敵敵畏 |
| dichlorvos,62-73-7,純度≥95% |
| 氯硝胺 |
| Dicloran,99-30-9,純度≥95% |
| 三氯殺螨醇 |
| Dicofol,115-32-2,純度≥95% |
| 樂果 |
| Dimethoate,60-51-5,純度≥95% |
| o,pˊ-滴滴滴 |
| 2,4ˊ-DDD;o,pˊ-DDD,53-19-0,純度≥95%,2,4ˊ-滴滴滴 |
| 敵噁磷 |
| Dioxathion,78-34-2,純度≥95% |
| 滅菌磷 |
| Ditalimfos,5131-24-8,純度≥95% |
| 敵瘟磷 |
| Edifenphos,17109-49-8,純度≥95% |
| 異狄氏劑 |
| Endrin,72-20-8,純度≥95% |
| 苯硫膦 |
| EPN,2104-64-5,純度≥95% |
| 氟環(huán)唑 |
| Epoxiconazole ,106325-08-0,純度≥95% |
| 乙丁烯氟靈 |
| Ethalfluralin,55283-68-6,純度≥95% |
| 滅線磷 |
| ethoprophos,13194-48-4,純度≥95% |
| 咪唑菌酮 |
| FENAMIDONE,161326-34-7,純度≥95% |
| 氯苯嘧啶醇 |
| Fenarimol ,60168-88-9,純度≥95% |
| 苯硫威 |
| fenothiocarb,62850-32-2,純度≥95% |
| 豐索磷 |
| Fensulfothion,115-90-2,純度≥95% |
| 倍硫磷 |
| Fenthion,55-38-9,純度≥95% |
| 氰戊菊酯 |
| fenvalerate,51630-58-1,純度≥95% |
| 氟酰胺 |
| Flutolanil,66332-96-5,純度≥95% |
| 地蟲硫磷 |
| Fonofos,944-22-9,純度≥95% |
| 安硫磷 |
| Formothion,2540-82-1,純度≥95% |
| 噻唑膦 |
| fosthiazate-1,純度≥95% |
| 六氯苯 |
| hexachlorobenzene,118-74-1,純度≥95% |
| 環(huán)嗪酮 |
| hexazinone,51235-04-2,純度≥95% |
| 抑霉唑 |
| Imazalil,35554-44-0,純度≥95% |
| 異稻瘟凈 |
| Iprobenfos,26087-47-8,純度≥95% |
| 異柳磷 |
| isofenphos,25311-71-1,純度≥95% |
| 甲基異柳磷 |
| Methyl isophenphos,99675-03-3,純度≥95% |
| 異丙威 |
| Isoprocarb,2631-40-5,純度≥95% |
| 噁唑啉 |
| oxazoline,27341-52-2,純度≥95% |
| 醚菌酯 |
| Kresoxim-methyl,143390-89-0,純度≥95% |
| 嘧菌胺 |
| Mepanipyrim,110235-47-7,純度≥95% |
| 地胺磷 |
| Mephosfolan,950-10-7,純度≥95% |
| 甲霜靈 |
| Metalaxyl,57837-19-1,純度≥95% |
| 蟲螨畏 |
| methacrifos,62610-77-9,純度≥95% |
| 甲胺磷 |
| Methamidophos,10265-92-6,純度≥95% |
| 異丙甲草胺 |
| metolachlor,51218-45-2,純度≥95% |
| 嗪草酮 |
| metribuzin,21087-64-9,純度≥95% |
| 速滅磷 |
| Mevinphos,7786-34-7,純度≥95% |
| 禾草敵 |
| Molinate,2212-67-1,純度≥95% |
| 久效磷 |
| Monocrotophos,6923-22-4,純度≥95% |
| o,pˊ-滴滴涕 |
| 2,4’-DDT,789-02-6,純度≥95%,2,4’-滴滴涕 |
| p,p’-滴滴滴 |
| 4,4′-DDD,72-54-8,純度≥95% |
| p,p’-滴滴伊 |
| 4,4’-滴滴伊,4,4’-DDE,72-55-9,純度≥95% |
| 噁草酮 |
| Oxadiazon,19666-30-9,純度≥95% |
| 乙氧氟草醚 |
| oxyflurofen,42874-03-3,純度≥95% |
| 對(duì)氧磷 |
| paraoxonethyl,311-45-5,純度≥95% |
| 甲基對(duì)氧磷 |
| Paraoxon-methyl,950-35-6,純度≥95% |
| 對(duì)硫磷 |
| Parathion,56-38-2,純度≥95% |
| 戊菌唑 |
| Penconazole,66246-88-6,純度≥95% |
| 氯菊酯 |
| permethrin-1,純度≥95% |
| 甲拌磷砜 |
| Phorate sulfone,2588-04-7,純度≥95% |
| 甲拌磷亞砜 |
| phoratesulfoxide,2588-03-6,純度≥95% |
| 增效醚 |
| piperonyl butoxide,51-03-6,純度≥95% |
| 哌草磷 |
| Piperophos,24151-93-7,純度≥95% |
| 抗蚜威 |
| Pirimicarb,23103-98-2,純度≥95% |
| 甲基嘧啶磷 |
| pirimiphosmethyl,29232-93-7,純度≥95% |
| 丙草胺 |
| Pretilachlor,51218-49-6,純度≥95% |
| 環(huán)丙氟靈 |
| Profluralin,26399-36-0,純度≥95% |
| 撲滅津 |
| propazine,139-40-2,純度≥95% |
| 胺丙畏 |
| propetamphos,31218-83-4,純度≥95% |
| 殘殺威 |
| Propoxur,114-26-1,純度≥95% |
| 吡菌磷 |
| Pyrazophos,13457-18-6,純度≥95% |
| 噠螨靈 |
| pyridaben,96489-71-3,純度≥95% |
| 吡丙醚 |
| pyriproxyfen,95737-68-1,純度≥95% |
| 喹硫磷 |
| Quinalphos,13593-03-8,純度≥95% |
| 喹氧靈 |
| quinoxyfen,124495-18-7,純度≥95% |
| 治螟磷 |
| sulfotep,3689-24-5,純度≥95% |
| 戊唑醇 |
| Tebuconazol,107534-96-3,純度≥95% |
| 吡螨胺 |
| Tebufenpyrad,119168-77-3,純度≥95% |
| 丁基嘧啶磷 |
| tebupirimfos,96182-53-5,純度≥95% |
| 特丁硫磷 |
| terbufos,13071-79-9,純度≥95% |
| 特丁硫磷砜 |
| terbufossulfone,56070-16-7,純度≥95% |
| 三氯殺螨砜 |
| Tetradifon,116-29-0,純度≥95% |
| 胺菊酯 |
| tetramethrin,純度≥95% |
| 禾草丹 |
| thiobencarb,28249-77-6,純度≥95% |
| 三唑酮 |
| triadimefon,43121-43-3,純度≥95% |
| 三唑醇 |
| Triadimenol,55219-65-3,純度≥95% |
| 野麥畏 |
| Tri-allate,2303-17-5,純度≥95% |
| 毒死蜱 |
| chlorpyrifos,2921-88-2,純度≥95% |
| 三唑磷 |
| triazophos,24017-47-8,純度≥95% |
| 肟菌酯 |
| Trifloxystrobin,141517-21-7,純度≥95% |
| 乙烯菌核利 |
| vinclozolin,50471-44-8,純度≥95% |
| 氟丙菊酯 |
| Acrinathrin,103833-18-7,純度≥95% |
| 艾氏劑 |
| Aldrin,309-00-2,純度≥95% |
| 莠滅凈 |
| Ametryn,834-12-8,純度≥95% |
| 阿特拉通 |
| Atratone,1610-17-9,純度≥95% |
| 莠去津 |
| atrazine,1912-24-9,純度≥95% |
| 益棉磷 |
| Azinphos-ethyl,2642-71-9,純度≥95% |
| 氟丁酰草胺 |
| BEFLUBUTAMID,113614-08-7,純度≥95% |
| 苯霜靈 |
| Benalaxyl,71626-11-4,純度≥95% |
| 乙丁氟靈 |
| Benfluralin,1861-40-1,純度≥95% |
| β-六六六 |
| β-HCB,319-85-7,純度≥95% |
| 甲羧除草醚 |
| Bifenox,42576-02-3,純度≥95% |
| 聯(lián)苯 |
| Biphenyl,92-52-4,純度≥95% |
| 乙基溴硫磷 |
| Bromophos-ethyl,4824-78-6,純度≥95% |
| 丁草胺 |
| butachlor,23184-66-9,純度≥95% |
| 抑草磷 |
| Butamifos,36335-67-8,純度≥95% |
| 克百威 |
| Carbofuran,1563-66-2,純度≥95% |
| 反式-氯丹 |
| TRANS-CHLORDANE,5103-74-2,純度≥95% |
| 殺螨酯 |
| chlorfenson,80-33-1,純度≥95% |
| 毒蟲畏 |
| Chlorfenvinphos,470-90-6,純度≥95% |
| 乙酯殺螨醇 |
| Chlorobenzilate,510-15-6,純度≥95% |
| 氯苯甲醚 |
| Chloroneb,2675-77-6,純度≥95% |
| 氯苯胺靈 |
| Chlorpropham,101-21-3,純度≥95% |
| 甲基毒死蜱 |
| Chlorpyrifos-methyl,5598-13-0,純度≥95% |
| 異噁草松 |
| Clomazone,81777-89-1,純度≥95%,異噁草酮 |
| 蠅毒磷 |
| coumaphos,56-72-4,純度≥95% |
| 氟氯氰菊酯 |
| cyfluthrin-1,純度≥95% |
| 環(huán)丙唑醇 |
| cyproconazole-1,純度≥95% |
| 嘧菌環(huán)胺 |
| Cyprodinil,121552-61-2,純度≥95% |
| δ-六六六 |
| δ-BHC,319-86-8,純度≥95% |
| 敵草凈 |
| oesmetryn,1014-69-3,純度≥95% |
| 二嗪磷 |
| Diazinon,333-41-5,純度≥95% |
| 禾草靈 |
| Diclofop-methyl,51338-27-3,純度≥95% |
| 百治磷 |
| dicrotophos,141-66-2,純度≥95% |
| 狄氏劑 |
| Dieldran,60-57-1,純度≥95% |
| 苯醚甲環(huán)唑 |
| difenoconazole-1,純度≥95% |
| 烯唑醇 |
| diniconazole,83657-24-3,純度≥95% |
| 二苯胺 |
| diphenylamin,122-39-4,純度≥95% |
| 異丙凈 |
| Dipropetryn,4147-51-7,純度≥95% |
| 硫草敵 |
| ETHIOLATE,2941-55-1,純度≥95% |
| 乙硫磷 |
| ethion,563-12-2,純度≥95% |
| 乙氧呋草黃 |
| ethofumesate,26225-79-6,純度≥95% |
| 乙螨唑 |
| Etoxazole,153233-91-1,純度≥95% |
| 土菌靈 |
| etridiazol,2593-15-9,純度≥95% |
| 乙嘧硫磷 |
| etrimfos,38260-54-7,純度≥95% |
| 伐滅磷 |
| Famphur,52-85-7,純度≥95% |
| 腈苯唑 |
| Fenbuconazole,114369-43-6,純度≥95% |
| 殺螟硫磷 |
| fenitrothion,122-14-5,純度≥95% |
| 仲丁威 |
| Fenobucarb,3766-81-2,純度≥95% |
| 甲氰菊酯 |
| fenpropathrin,64257-84-7,純度≥95% |
| 倍硫磷砜 |
| Fenthionsulfone,3761-42-0,純度≥95% |
| 倍硫磷亞砜 |
| Fenthionsulfoxide,3761-41-9,純度≥95% |
| 氟蟲腈 |
| fipronil,120068-37-3,純度≥95% |
| 吡氟禾草靈 |
| fluazifopbutyl,69806-50-4,純度≥95% |
| 氟氰戊菊酯 |
| flucythrinate,70124-77-5,純度≥95% |
| 咯菌腈 |
| Fludioxonil,131341-86-1,純度≥95% |
| 三氟硝草醚 |
| Fluorodifen,15457-05-3,純度≥95% |
| 氟喹唑 |
| Fluquinconazole,136426-54-5,純度≥95% |
| 氟胺氰菊酯 |
| tau－fluvalinate ,102851-06-9 ,純度≥95% |
| γ-六六六 |
| γ-HCB,58-89-9,純度≥95% |
| 己唑醇 |
| Hexaconazole,79983-71-4,純度≥95% |
| 異菌脲 |
| iprodione,36734-19-7,純度≥95% |
| 氯唑磷 |
| isazofos,42509-80-8,純度≥95% |
| 水胺硫磷 |
| Isocarbophos,24353-61-5,純度≥95% |
| 氧異柳磷 |
| Isofenphos oxon,31120-85-1,純度≥95% |
| 稻瘟靈 |
| isoprothiolane,50512-35-1,純度≥95% |
| 高效氯氟氰菊酯 |
| iambda-cyhalothrin,純度≥95% |
| 溴苯磷 |
| leptomycin b,21609-90-5,純度≥95%,溴苯膦 |
| 馬拉氧磷 |
| malaoxon,1634-78-2,純度≥95% |
| 馬拉硫磷 |
| malathion,121-75-5,純度≥95% |
| 苯噻酰草胺 |
| mefenacet,73250-68-7,純度≥95% |
| 殺撲磷 |
| methidathion,950-37-8,純度≥95% |
| 烯蟲酯 |
| Methoprene,40596-69-8,純度≥95% |
| o,p’-滴滴伊 |
| 2,4’-DDE,3424-82-6,純度≥95%,2,4’-滴滴伊 |
| p,p’-滴滴伊 |
| 4,4’-滴滴伊4,4’-DDE,72-55-9,純度≥95%,4,4’-滴滴伊 |
| 甲氧滴滴涕 |
| Methoxychlor,72-43-5,純度≥95% |
| 綠谷隆 |
| monolinuron,1746-81-2,純度≥95% |
| 腈菌唑 |
| Myclobutanil,88671-89-0,純度≥95% |
| 二溴磷 |
| DIBROM ,300-76-5,純度≥95% |
| 敵草胺 |
| napropamide,15299-99-7,純度≥95% |
| 除草醚 |
| Nitrofen,1836-75-5,純度≥95% |
| 氧樂果 |
| omethoate,1113-02-6,純度≥95% |
| 噁霜靈 |
| Oxadixyl,77732-09-3,純度≥95% |
| 多效唑 |
| paclobutrazol,76738-62-0,純度≥95% |
| 甲基對(duì)硫磷 |
| methylparathion,298-00-0,純度≥95% |
| 二甲戊靈 |
| pendimethalin,40487-42-1,純度≥95% |
| 五氯苯胺 |
| Pentachloroaniline,527-20-8,純度≥95% |
| 五氯硝基苯 |
| quintozene,82-68-8,純度≥95% |
| 甲拌磷 |
| phorate,298-02-2,純度≥95% |
| 伏殺硫磷 |
| phosalone,2310-17-0,純度≥95% |
| 硫環(huán)磷 |
| phosfolan,947-02-4,純度≥95% |
| 亞胺硫磷 |
| Phosmet,732-11-6,純度≥95% |
| 磷胺 |
| Phosphamidon,純度≥95% |
| 嘧啶磷 |
| pyrimitate,23505-41-1,純度≥95% |
| 腐霉利 |
| procymidone,32809-16-8,純度≥95% |
| 丙溴磷 |
| profenefos,41198-08-7,純度≥95% |
| 撲草凈 |
| Prometryn,7287-19-6,純度≥95% |
| 炔苯酰草胺 |
| Propyzamide,23950-58-5,純度≥95% |
| 敵稗 |
| propanil,709-98-8,純度≥95% |
| 殺蟲畏 |
| tetrachlorvinphos,22248-79-9,純度≥95% |
| 丙環(huán)唑 |
| propiconazole-1,純度≥95% |
| 四氟醚唑 |
| tetraconazole,112281-77-3,純度≥95% |
| 丙硫磷 |
| Prothiophos,34643-46-4,純度≥95% |
| 噠嗪硫磷 |
| pyridaphenthion,119-12-0,純度≥95% |
| 蟲線磷 |
| Thionazin,297-97-2,純度≥95% |
| 甲基立枯磷 |
| Tolclofos-methyl,57018-04-9,純度≥95% |
| 嘧霉胺 |
| Pyrimethanil,53112-28-0,純度≥95% |
| 毒壤膦 |
| Trichloronat,327-98-0,純度≥95% |
| 皮蠅磷 |
| ronnel(fenchlorphos),299-84-3,純度≥95% |
| 西瑪津 |
| Simazine,122-34-9,純度≥95% |
| 四氯硝基苯 |
| Tecnazene,117-18-0,純度≥95% |
| 特丁津 |
| terbuthylazine,5915-41-3,純度≥95% |
| 特丁凈 |
| terbutryn,886-50-0,純度≥95% |
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