{"id":5545,"date":"2024-04-24T10:01:40","date_gmt":"2024-04-24T02:01:40","guid":{"rendered":"https:\/\/www.chector.com\/?p=5545"},"modified":"2024-04-24T10:10:30","modified_gmt":"2024-04-24T02:10:30","slug":"shi-pin-zhong-zhi-fang-suan-de-ce-ding-yi-qi-hao-cai-pei-zhi-qing-dan","status":"publish","type":"post","link":"https:\/\/www.chector.com\/news\/ntypes\/food\/shi-pin-zhong-zhi-fang-suan-de-ce-ding-yi-qi-hao-cai-pei-zhi-qing-dan.html","title":{"rendered":"GB 5009.168-2016\u98df\u54c1\u4e2d\u8102\u80aa\u9178\u7684\u6d4b\u5b9a\u4eea\u5668\u8017\u6750\u914d\u7f6e\u6e05\u5355"},"content":{"rendered":"\n
\"\"<\/a><\/figure>
\n

\u66ff\u4ee3\u6807\u51c6\uff1aGB\/T 5009.168-2003,GB 5413.27\uff1b\u672c\u6807\u51c6\u89c4\u5b9a\u4e86\u98df\u54c1\u4e2d\u8102\u80aa\u9178\u542b\u91cf\u7684\u6d4b\u5b9a\u65b9\u6cd5\u3002\u672c\u6807\u51c6\u9002\u7528\u4e8e\u98df\u54c1\u4e2d\u603b\u8102\u80aa\ufe51\u9971\u548c\u8102\u80aa(\u9178)\u3001\u4e0d\u9971\u548c\u8102\u80aa(\u9178)\u7684\u6d4b\u5b9a\u3002\u672c\u6807\u51c6\u4e2d\u6c34\u89e3\u63d0\u53d6\u6cd5\u9002\u7528\u4e8e\u98df\u54c1\u4e2d\u8102\u80aa\u9178\u542b\u91cf\u7684\u6d4b\u5b9a:\u916f\u4ea4\u6362\u6cd5\u9002\u7528\u4e8e\u6e38\u79bb\u8102\u80aa\u9178\u542b\u91cf\u4e0d\u5927\u4e8e2\uff05\u7684\u6cb9\u8102\u6837\u54c1\u7684\u8102\u80aa\u9178\u542b\u91cf\u6d4b\u5b9a\uff1b\u4e59\u9170\u6c2f-\u7532\u9187\u6cd5\u9002\u7528\u4e8e\u542b\u6c34\u91cf\u5c0f\u4e8e5\uff05\u7684\u4e73\u7c89\u548c\u65e0\u6c34\u5976\u6cb9\u6837\u54c1\u7684\u8102\u80aa\u9178\u542b\u91cf\u6d4b\u5b9a\u3002\uff08\u70b9\u51fb\u56fe\u7247\u67e5\u770b\u6807\u51c6\u8be6\u60c5\uff09<\/strong><\/p>\n<\/div><\/div>\n\n\n\n

\u7b2c\u4e00\u6cd5 \u5185\u6807\u6cd5<\/p>\n\n\n\n

\u539f\u7406:2.1\u6c34\u89e3\u63d0\u53d6\u6cd5:\u52a0\u5165\u5185\u6807\u7269\u7684\u8bd5\u6837\u7ecf\u6c34\u89e3\u4e59\u919a\u6eb6\u6db2\u63d0\u53d6\u5176\u4e2d\u7684\u8102\u80aa\u540e\uff0c\u5728\u78b1\u6027\u6761\u4ef6\u4e0b\u7682\u5316\u548c\u7532\u916f\u5316\uff0c\u751f\u6210\u8102\u80aa\u9178\u7532\u916f,\u7ecf\u6bdb\u7ec6\u7ba1\u67f1\u6c14\u76f8\u8272\u8c10\u5206\u6790\uff0c\u5185\u6807\u6cd5\u5b9a\u91cf\u6d4b\u5b9a\u8102\u80aa\u9178\u7532\u916f\u542b\u91cf\u3002\u4f9d\u636e\u5404\u79cd\u8102\u80aa\u9178\u7532\u916f\u542b\u91cf\u548c\u8f6c\u6362\u7cfb\u6570\u8ba1\u7b97\u51fa\u603b\u8102\u80aa,\u9971\u548c\u8102\u80aa(\u9178)\u3001\u5355\u4e0d\u9971\u548c\u8102\u80aa(\u9178)\u3001\u591a\u4e0d\u9971\u548c\u8102\u80aa(\u9178)\u542b\u91cf\u3002<\/p>\n\n\n\n

\u52a8\u690d\u7269\u6cb9\u8102\u8bd5\u6837\u4e0d\u7ecf\u8102\u80aa\u63d0\u53d6,\u52a0\u5165\u5185\u6807\u7269\u540e\u76f4\u63a5\u8fdb\u884c\u7682\u5316\u548c\u8102\u80aa\u9178\u7532\u916f\u5316\u3002<\/p>\n\n\n\n

2.2\u916f\u4ea4\u6362\u6cd5(\u9002\u7528\u4e8e\u6e38\u79bb\u8102\u80aa\u9178\u542b\u91cf\u4e0d\u5927\u4e8e2%\u7684\u6cb9\u8102):\u5c06\u6cb9\u8102\u6eb6\u89e3\u5728\u5f02\u8f9b\u70f7\u4e2d,\u52a0\u4eba\u5185\u6807\u7269\u540e,\u52a0\u5165\u6c22\u6c27\u5316\u94be\u7532\u9187\u6eb6\u6db2\u901a\u8fc7\u916f\u4ea4\u6362\u7532\u916f\u5316\uff0c\u53cd\u5e94\u5b8c\u5168\u540e,\u7528\u786b\u9178\u6c22\u94a0\u4e2d\u548c\u5269\u4f59\u6c22\u6c27\u5316\u94be.\u4ee5\u907f\u514d\u7532\u916f\u7682\u5316\u3002<\/p>\n\n\n\n

\u6c34<\/td><\/tr>
\u4e3aGB\/T 6682\u89c4\u5b9a\u7684\u4e00\u7ea7\u6c34<\/td><\/tr>
\u76d0\u9178<\/td><\/tr>
HCl\uff0c\u5206\u6790\u7eaf<\/td><\/tr>
\u6c28\u6c34<\/td><\/tr>
NH3\u00b7H2O\uff0c\u5206\u6790\u7eaf<\/td><\/tr>
\u7126\u6027\u6ca1\u98df\u5b50\u9178<\/td><\/tr>
C6H6O3\uff0c\u5206\u6790\u7eaf<\/td><\/tr>
\u4e59\u919a<\/td><\/tr>
C4H10O\uff0c\u5206\u6790\u7eaf<\/td><\/tr>
\u77f3\u6cb9\u919a<\/td><\/tr>
\u6cb8\u7a0b30\u2103~60\u2103<\/td><\/tr>
\u4e59\u9187<\/td><\/tr>
C2H6O\uff0c95%\uff0c\u5206\u6790\u7eaf<\/td><\/tr>
\u7532\u9187<\/td><\/tr>
CH3OH\uff0c\u8272\u8c31\u7eaf<\/td><\/tr>
\u6c22\u6c27\u5316\u94a0<\/td><\/tr>
NaOH\uff0c\u5206\u6790\u7eaf<\/td><\/tr>
\u6b63\u5e9a\u70f7<\/td><\/tr>
[CH3(CH2)5CH3]\uff0c\u8272\u8c31\u7eaf<\/td><\/tr>
\u786b\u9178\u94a0<\/td><\/tr>
\u65e0\u6c34\u786b\u9178\u94a0,Na2SO4\uff0c\u5206\u6790\u7eaf<\/td><\/tr>
\u6c2f\u5316\u94a0<\/td><\/tr>
NaCl\uff0c\u5206\u6790\u7eaf<\/td><\/tr>
\u7532\u9187<\/td><\/tr>
–<\/td><\/tr>
\u6c22\u6c27\u5316\u94a0<\/td><\/tr>
–<\/td><\/tr>
\u6df7\u5408\u8102\u80aa\u9178\u7532\u916f\u6807\u51c6\u6eb6\u6db2<\/td><\/tr>
\u6df7\u5408\u8102\u80aa\u9178\u7532\u916f\u6807\u51c6\u54c1<\/td><\/tr>
\u5f02\u8f9b\u70f7<\/td><\/tr>
[(CH3)2CHCH2C(CH3)3]\uff0c\u8272\u8c31\u7eaf<\/td><\/tr>
\u786b\u9178\u6c22\u94a0<\/td><\/tr>
NaHSO4\uff0c\u5206\u6790\u7eaf<\/td><\/tr>
\u6c22\u6c27\u5316\u94be<\/td><\/tr>
KOH\uff0c\u5206\u6790\u7eaf<\/td><\/tr>
\u5341\u4e00\u78b3\u9178\u7518\u6cb9\u4e09\u916f<\/td><\/tr>
(C36H68O6,CAS\u53f7:13552-80-2)<\/td><\/tr>
\u70e7\u676f<\/td><\/tr>
–<\/td><\/tr>
\u5bb9\u91cf\u74f6<\/td><\/tr>
500ml<\/td><\/tr>
\u5bb9\u91cf\u74f6<\/td><\/tr>
10ml<\/td><\/tr>
\u51b0\u7bb1<\/td><\/tr>
-10 \u2103<\/td><\/tr>
\u5300\u6d46\u673a<\/td><\/tr>
\u6216\u5b9e\u9a8c\u5ba4\u7528\u7ec4\u7ec7\u7c89\u788e\u673a\u6216\u7814\u78e8\u673a<\/td><\/tr>
\u6c14\u76f8\u8272\u8c31\u4eea<\/td><\/tr>
\u5177\u6709\u6c22\u706b\u7130\u79bb\u5b50\u68c0\u6d4b\u5668(FID)<\/td><\/tr>
\u6c14\u76f8\u8272\u8c31\u67f1<\/td><\/tr>
\u805a\u4e8c\u6c30\u4e19\u57fa\u7845\u6c27\u70f7\u5f3a\u6781\u6027\u56fa\u5b9a\u76f8\u6bdb\u7ec6\u7ba1\u8272\u8c31\u67f1\uff0c\u67f1\u957f100m,\u5185\u5f840.25mm,\u819c\u539a0.2\u03bcm<\/td><\/tr>
\u6c34\u6d74\u7bb1<\/td><\/tr>
\u6052\u6e29\u6c34\u6d74\uff0c\u63a7\u6e29\u8303\u56f440\u2103~100\u2103,\u63a7\u6e29\u00b11\u2103<\/td><\/tr>
\u5929\u5e73<\/td><\/tr>
\u5206\u6790\u5929\u5e73\uff0c\u611f\u91cf0.1mg<\/td><\/tr>
\u65cb\u8f6c\u84b8\u53d1\u4eea<\/td><\/tr>
–<\/td><\/tr>
\u70e7\u74f6<\/td><\/tr>
\u5e73\u5e95\uff0c250ml<\/td><\/tr>
\u6cb8\u77f3<\/td><\/tr>
–<\/td><\/tr>
\u5206\u6db2\u6f0f\u6597<\/td><\/tr>
–<\/td><\/tr>
\u56de\u6d41\u51b7\u51dd\u88c5\u7f6e<\/td><\/tr>
\u56de\u6d41\u51b7\u51dd\u5668<\/td><\/tr>
\u8bd5\u7ba1<\/td><\/tr>
25ml<\/td><\/tr>
\u8bd5\u7ba1<\/td><\/tr>
\u5177\u585e<\/td><\/tr>
\u6c2e\u6c14<\/td><\/tr>
\u8f7d\u6c14<\/td><\/tr><\/tbody><\/table>
\u4ea7\u54c1\u6e05\u5355<\/figcaption><\/figure>\n\n\n\n

\u7b2c\u4e8c\u6cd5 \u5916\u6807\u6cd5<\/p>\n\n\n\n

\u539f\u7406:\u6c34\u89e3-\u63d0\u53d6\u6cd5:\u8bd5\u6837\u7ecf\u6c34\u89e3-\u4e59\u919a\u6eb6\u6db2\u63d0\u53d6\u5176\u4e2d\u7684\u8102\u80aa\u540e,\u5728\u78b1\u6027\u6761\u4ef6\u4e0b\u7682\u5316\u548c\u7532\u916f\u5316\uff0c\u751f\u6210\u8102\u80aa\u9178\u7532\u916f,\u7ecf\u6bdb\u7ec6\u7ba1\u67f1\u6c14\u76f8\u8272\u8c31\u5206\u6790,\u5916\u6807\u6cd5\u5b9a\u91cf\u6d4b\u5b9a\u8102\u80aa\u9178\u7684\u542b\u91cf\u3002<\/p>\n\n\n\n

\u52a8\u690d\u7269\u7eaf\u6cb9\u8102\u8bd5\u6837\u4e0d\u7ecf\u8102\u80aa\u63d0\u53d6,\u76f4\u63a5\u8fdb\u884c\u7682\u5316\u548c\u8102\u80aa\u9178\u7532\u916f\u5316\u3002<\/p>\n\n\n\n

\u4e59\u9170\u6c2f-\u7532\u9187\u6cd5(\u9002\u7528\u4e8e\u542b\u6c34\u91cf\u5c0f\u4e8e5%\u7684\u4e73\u7c89\u548c\u65e0\u6c34\u5976\u6cb9\u8bd5\u6837):\u4e59\u9170\u6c2f\u4e0e\u7532\u9187\u53cd\u5e94\u5f97\u5230\u7684\u76d0\u9178-\u7532\u9187\u4f7f\u5176\u4e2d\u7684\u8102\u80aa\u548c\u6e38\u79bb\u8102\u80aa\u9178\u7532\u916f\u5316,\u7528\u7532\u82ef\u63d0\u53d6\u540e,\u7ecf\u6c14\u76f8\u8272\u8c31\u4eea\u5206\u79bb\u68c0\u6d4b,\u5916\u6807\u6cd5\u5b9a\u91cf\u3002<\/p>\n\n\n\n

\u916f\u4ea4\u6362\u6cd5(\u9002\u7528\u4e8e\u6e38\u79bb\u8102\u80aa\u9178\u542b\u91cf\u4e0d\u5927\u4e8e2%\u7684\u6cb9\u8102):\u5c06\u6cb9\u8102\u6eb6\u89e3\u5728\u5f02\u8f9b\u70f7\u4e2d,\u52a0\u4eba\u6c22\u6c27\u5316\u94be\u7532\u9187\u6eb6\u6db2\u901a\u8fc7\u916f\u4ea4\u6362\u7532\u916f\u5316.\u53cd\u5e94\u5b8c\u5168\u540e,\u7528\u786b\u9178\u6c22\u94a0\u4e2d\u548c\u5269\u4f59\u6c22\u6c27\u5316\u94be.\u5916\u6807\u6cd5\u5b9a\u91cf\u6d4b\u5b9a\u8102\u80aa\u9178\u7684\u542b\u91cf\u3002<\/p>\n\n\n\n

\u6c34<\/td><\/tr>
\u4e3aGB\/T 6682\u89c4\u5b9a\u7684\u4e00\u7ea7\u6c34<\/td><\/tr>
\u76d0\u9178<\/td><\/tr>
HCl\uff0c\u5206\u6790\u7eaf<\/td><\/tr>
\u6df7\u5408\u8102\u80aa\u9178\u7532\u916f\u6807\u51c6\u6eb6\u6db2<\/td><\/tr>
–<\/td><\/tr>
\u987a,\u987a-9,12-\u5341\u516b\u78b3\u4e8c\u70ef\u9178\u7532\u916f<\/td><\/tr>
\u8102\u80aa\u9178\u7518\u6cb9\u4e09\u916f\u6807\u51c6\u54c1.\u7eaf\u5ea6\u226599%<\/td><\/tr>
\u6c28\u6c34<\/td><\/tr>
NH3\u00b7H2O\uff0c\u5206\u6790\u7eaf<\/td><\/tr>
\u7126\u6027\u6ca1\u98df\u5b50\u9178<\/td><\/tr>
C6H6O3\uff0c\u5206\u6790\u7eaf<\/td><\/tr>
\u4e59\u919a<\/td><\/tr>
C4H10O\uff0c\u5206\u6790\u7eaf<\/td><\/tr>
\u77f3\u6cb9\u919a<\/td><\/tr>
\u6cb8\u7a0b30\u2103~60\u2103<\/td><\/tr>
\u4e59\u9187<\/td><\/tr>
(C2H6O)(95%),\u5206\u6790\u7eaf<\/td><\/tr>
\u7532\u9187<\/td><\/tr>
CH3OH\uff0c\u8272\u8c31\u7eaf<\/td><\/tr>
\u6c22\u6c27\u5316\u94a0<\/td><\/tr>
NaOH\uff0c\u5206\u6790\u7eaf<\/td><\/tr>
\u6b63\u5e9a\u70f7<\/td><\/tr>
[CH3(CH2)5CH3]\uff0c\u8272\u8c31\u7eaf<\/td><\/tr>
\u4e09\u6c1f\u5316\u787c<\/td><\/tr>
BF3,7637-07-2<\/td><\/tr>
\u786b\u9178\u94a0<\/td><\/tr>
\u65e0\u6c34\u786b\u9178\u94a0,Na2SO4\uff0c\u5206\u6790\u7eaf<\/td><\/tr>
\u6c2f\u5316\u94a0<\/td><\/tr>
NaCl\uff0c\u5206\u6790\u7eaf<\/td><\/tr>
\u78b3\u9178\u94a0<\/td><\/tr>
\u65e0\u6c34\u78b3\u9178\u94a0,Na2CO3\uff0c\u5206\u6790\u7eaf<\/td><\/tr>
\u7532\u82ef<\/td><\/tr>
C7H8\uff0c\u8272\u8c31\u7eaf<\/td><\/tr>
\u4e59\u9170\u6c2f<\/td><\/tr>
C2H3ClO\uff0c\u5206\u6790\u7eaf<\/td><\/tr>
\u5f02\u8f9b\u70f7<\/td><\/tr>
[(CH3)2CHCH2C(CH3)3]\uff0c\u8272\u8c31\u7eaf<\/td><\/tr>
\u786b\u9178\u6c22\u94a0<\/td><\/tr>
NaHSO4\uff0c\u5206\u6790\u7eaf<\/td><\/tr>
\u6c22\u6c27\u5316\u94be<\/td><\/tr>
KOH\uff0c\u5206\u6790\u7eaf<\/td><\/tr>
\u70e7\u676f<\/td><\/tr>
100ml<\/td><\/tr>
\u5bb9\u91cf\u74f6<\/td><\/tr>
50ml<\/td><\/tr>
\u5bb9\u91cf\u74f6<\/td><\/tr>
100ml<\/td><\/tr>
\u51b0\u7bb1<\/td><\/tr>
-10 \u2103<\/td><\/tr>
\u5300\u6d46\u673a<\/td><\/tr>
\u6216\u5b9e\u9a8c\u5ba4\u7528\u7ec4\u7ec7\u7c89\u788e\u673a\u6216\u7814\u78e8\u673a<\/td><\/tr>
\u6c14\u76f8\u8272\u8c31\u4eea<\/td><\/tr>
\u5177\u6709\u6c22\u706b\u7130\u79bb\u5b50\u68c0\u6d4b\u5668(FID)<\/td><\/tr>
\u6c14\u76f8\u8272\u8c31\u67f1<\/td><\/tr>
\u805a\u4e8c\u6c30\u4e19\u57fa\u7845\u6c27\u70f7\u5f3a\u6781\u6027\u56fa\u5b9a\u76f8\u6bdb\u7ec6\u7ba1\u8272\u8c31\u67f1\uff0c\u67f1\u957f100m,\u5185\u5f840.25mm,\u819c\u539a0.2\u03bcm<\/td><\/tr>
\u6c34\u6d74\u7bb1<\/td><\/tr>
\u6052\u6e29\u6c34\u6d74\uff0c\u63a7\u6e29\u8303\u56f440\u2103~100\u2103,\u63a7\u6e29\u00b11\u2103<\/td><\/tr>
\u5929\u5e73<\/td><\/tr>
\u5206\u6790\u5929\u5e73\uff0c\u611f\u91cf0.1mg<\/td><\/tr>
\u79bb\u5fc3\u673a<\/td><\/tr>
\u8f6c\u901f\u22655000r\/min<\/td><\/tr>
\u65cb\u8f6c\u84b8\u53d1\u4eea<\/td><\/tr>
–<\/td><\/tr>
\u73bb\u7483\u7ba1<\/td><\/tr>
\u87ba\u53e3\uff0c\u5e26\u6709\u805a\u56db\u6c1f\u4e59\u70ef\u505a\u5185\u57ab\u7684\u87ba\u53e3\u76d6\uff0c15mL<\/td><\/tr>
\u79bb\u5fc3\u7ba1<\/td><\/tr>
50mL<\/td><\/tr>
\u70e7\u74f6<\/td><\/tr>
\u5e73\u5e95<\/td><\/tr>
\u6cb8\u77f3<\/td><\/tr>
–<\/td><\/tr>
\u8bd5\u7ba1<\/td><\/tr>
\u5177\u585e<\/td><\/tr>
\u6c34<\/td><\/tr>
\u4e3aGB\/T 6682\u89c4\u5b9a\u7684\u4e00\u7ea7\u6c34<\/td><\/tr>
\u70e7\u74f6<\/td><\/tr>
\u5e73\u5e95\uff0c250ml<\/td><\/tr>
\u6df7\u5408\u8102\u80aa\u9178\u7532\u916f\u6807\u51c6\u6eb6\u6db2<\/td><\/tr>
–<\/td><\/tr>
\u6cb8\u77f3<\/td><\/tr>
–<\/td><\/tr>
\u8bd5\u7ba1<\/td><\/tr>
\u5177\u585e<\/td><\/tr><\/tbody><\/table>
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C20:3n3 ,C21H36O2 ,55682-88-7<\/td><\/tr>
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C20:4n6 ,C21H34O2,2566-89-4<\/td><\/tr>
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C20:5n3 ,C21H32O2, 2734-47-6<\/td><\/tr>
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